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Structure of 2,6- Dinitrophenylsulfanyl-ethanenitrile and 2,4,6-Trinitrophenylsulfanylethanenitrile and Their Ring Closure Giving 2-Cyanobenzo[d]thiazole-3-oxides
Authors: Černý Jiří | Bertolasi Valerio | Hanusek Jiří | Macháček Vladimír
Year: 2008
Type of publication: článek v odborném periodiku
Name of source: Heterocycles
Publisher name: The Japan Institute of Heterocyclic Chemistry
Place: Tokyo
Page from-to: 1425-1433
Titles:
Language Name Abstract Keywords
cze Struktura 2,6-dinitrofenylsulfanylethannitrilu a 2,4,6-trinitrofenylsulfanylethannitrilu a jejich cyklizace poskytující 2-kyanbenzo[d]thiazol-3-oxidy Bazicky katalyzovaná cyklizace 2,6-dinitrofenylsulfanylethannitrilu a 2,4,6-trinitrofenylsulfanylethannitrilu poskytuje 2-kyan-7-nitrobenzo[d]thiazol-3-oxid a 2-kyan-5,7-dinitrobenzo[d]thiazol-3-oxid. Struktura výchozích fenylsulfanyl-ethannitrilů byla studována jak v krystalu tak i v roztoku.
eng Structure of 2,6- Dinitrophenylsulfanyl-ethanenitrile and 2,4,6-Trinitrophenylsulfanylethanenitrile and Their Ring Closure Giving 2-Cyanobenzo[d]thiazole-3-oxides The base-catalysed ring closure of 2,6-dinitrophenylsulfanylethanenitrile and 2,4,6-trinitrophenyl-sulfanylethanenitrile gives 2-cyano-7-nitrobenzo[d]thiazole-3-oxide and 2-cyano-5,7-dinitrobenzo[d]thiazole-3-oxide, respectively. Structure of the starting phenylsulfanyl-ethanenitriles has been studied both in crystal and in solution. 2,6-dinitrophenylsulfanylethanenitrile, 2,4,6-trinitrophenylsulfanylethanenitrile, 2-cyano-7-nitrobenzo[d]thiazole-3-oxide, 2-cyano-5,7-dinitrobenzo[d]thiazole-3-oxide, X-ray, NMR.

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