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Combined Kinetic Analysis for Crystallization Kinetics of Non-crystalline Solids
Authors: Pérez-Maqueda L. A. | Criado J. M. | Málek Jiří
Year: 2003
Type of publication: článek v odborném periodiku
Name of source: Journal of Non-Crystalline Solids
Publisher name: Elsevier Science BV
Place: Amsterdam
Page from-to: 84-91
Titles:
Language Name Abstract Keywords
cze Combined Kinetic Analysis for Crystallization Kinetics of Non-crystalline Solids A new method of kinetic analysis that allows the combined analysis of data obtained under different experimental conditions, i. e. heating pathway, is presented for the crystallization of non-crystalline solids. The method consists of a two-stage procedure. Firstly, an optimization procedure is applied for the determination of the Johnson, Mehl and Avrami (JMA). This optimization procedure is based on the linearization of the rate equation throw a logarithmic transformation; where the correlation coefficient function is the objective function, and the JMA order is the adjustable parameter. The JMA order obtained from this optimization procedure allows one to determine in a second stage the other kinetic parameters. crystallization kinetics of non-crystalline solids
eng Combined Kinetic Analysis for Crystallization Kinetics of Non-crystalline Solids A new method of kinetic analysis that allows the combined analysis of data obtained under different experimental conditions, i. e. heating pathway, is presented for the crystallization of non-crystalline solids. The method consists of a two-stage procedure. Firstly, an optimization procedure is applied for the determination of the Johnson, Mehl and Avrami (JMA). This optimization procedure is based on the linearization of the rate equation throw a logarithmic transformation; where the correlation coefficient function is the objective function, and the JMA order is the adjustable parameter. The JMA order obtained from this optimization procedure allows one to determine in a second stage the other kinetic parameters. crystallization kinetics of non-crystalline solids

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