Publication detail

Determination of Extraframework Metal Content in Zeolitic Catalysts by Means of WD XRF Spectrometry

Authors: Knotek Petr | Pouzar Miloslav | Bulánek Roman | Novoveská Kateřina

Year: 2003

Type of publication: článek v odborném periodiku

Name of source: Scientific Papers of the University of Pardubice, Series A, Faculty of Chemical Technology

Publisher name: Univerzita Pardubice

Place: Pardubice

Page from-to: 97-114

Titles:

Language	Name	Abstract	Keywords
cze			xxx
eng	Determination of Extraframework Metal Content in Zeolitic Catalysts by Means of WD XRF Spectrometry	XRF spectroscopy is not widely used for zeolites analysis, but its known advantages are indispensable i.e. small consumption of the sample (5 mg), analysis of the sample without dissolution, quickly and easy pre-treatment and low-cost analysis. Therefore, development of methodology for determination of metal (Cu, Co, Ga, V) content in zeolites using wavelength dispersive X-ray fluorescence analysis is described in this paper. XRF spectrometer was calibrated for each metal using model pellets containing oxide and boric acid. Response of detector on the amount of metal can be reliable fitted by linear model. Copper (resp. cobalt) zeolites showed good agreement in metal content determination by XRF and standard validated analysis (AAS and ICP-OES after zeolite dissolution).	XRF spectroscopy, zeolites, catalysts

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