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[2-((R)-{2-[(S)-1-Benzylpyrrolidin-2-yl-carbonylazanidyl]phenyl}(phenyl)methylideneamino)-4-hydroxybutanoato-kappa(4)N,N '',N '',O(1)]nickel(II) toluene disolvate
Authors: Padělková Zdeňka | Popkov Alexander | Nádvorník Milan
Year: 2011
Type of publication: článek v odborném periodiku
Name of source: Acta Crystallographica Section E - Structure Reports Online
Publisher name: International Union of Crystallography
Page from-to: m1258-u940
Titles:
Language Name Abstract Keywords
cze [2-((R)-{2-[(S)-1-Benzylpyrrolidin-2-yl-karbonylazanidyl]fenyl}(fenyl)methylideneamino)-4-hydroxybutanoato-kappa(4)N,N '',N '',O(1)]nikl(II) toluen disolvát Kolem centálního atomu Ni ve studované sloučenině [Ni(C(29)H(29-)N(3)O(4))] 2C(7)H(8) je uspořádání koordinačního okolí čtvercově planární se třemi atomy N [Ni-N = 1.942 (3), 1.843 (3) a 1.853 (3) angstrom] a jedním atomem O [1.868 (3) angstrom] y tetradentátního ligandu. Uspořádání hydroxybutanoátů do řetězců je způsobeno díky intermolekulárním vodíkovým vazbám. X-ray;Ni komplex
eng [2-((R)-{2-[(S)-1-Benzylpyrrolidin-2-yl-carbonylazanidyl]phenyl}(phenyl)methylideneamino)-4-hydroxybutanoato-kappa(4)N,N '',N '',O(1)]nickel(II) toluene disolvate The central Ni atom in the title compound, [Ni(C(29)H(29-)N(3)O(4))]center dot 2C(7)H(8), is coordinated in a distorted square-planar environment by three N atoms [Ni-N = 1.942 (3), 1.843 (3) and 1.853 (3) angstrom] and one O atom [1.868 (3) angstrom] of the tetradentate ligand. The conformation of the hydroxybutanoate side chain is controlled by an intermolecular hydrogen bond. X-ray;Ni complex

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