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Supercritical CO2 Extraction of Volatiles from Rose Petals
Authors: Surmová Silvie | Eisner Aleš | Kašparová Pavla | Ventura Karel
Year: 2016
Type of publication: ostatní - článek ve sborníku
Name of source: 31st International Symposium on Chromatography : congress proceedings
Publisher name: Apryll M. Stalcup and Jeremy D. Glennon
Place: Cork
Page from-to: 368-368
Titles:
Language Name Abstract Keywords
eng Supercritical CO2 Extraction of Volatiles from Rose Petals Among the different extraction techniques used at analytical and preparative scale, supercritical fluid extraction is one of the most used, especially for natural products. This paper describes extraction of volatiles from rose petals using supercritical fluid extraction (CO2) and following gas chromatography mass spectrometry analysis. This work was focus on finding the optimized conditions of extraction of volatiles and identification with the largest number of compounds. Different parameters including extraction pressure (116–384 bar), extraction temperature (36.50–103.5 °C) and volume of carbon dioxide (990 mL–6010 mL) with CO2 flow rate 80-120 mL/min and polar modifier (methanol, acetonitrile and toluene), were investigated. Extraction solution, such as toluene, hexane, methanol, were also studied and results were compared. SFE; Rose Petals; GC-MS