Publication detail

Synthesis of 2,2-dinitroethene-1,1-diamine from 2 methylpyrimidine-4,6-diol and treatment of the dinitromethane produced

Year: 2018

Type of publication: článek ve sborníku

Name of source: Proceedings of the 21st Seminar on New Trends in Research of Energetic Materials

Publisher name: Univerzita Pardubice

Place: Pardubice

Page from-to: 703-712

Titles:

Language	Name	Abstract	Keywords
cze	Příprava 2,2-dinitroethen-1,1-diaminu z 2-methylpyrimidin-4,6-diola a možnosti dinitromethanu of the dinitromethane produced Příprava 2,2-dinitroethen-1,1-diaminu z 2 methylpyrimidin-4,6-diolu and treatment of the dinitromethane produced	2,2-Dinitroethene-1,1-diamin (FOX-7) byl připraven z 2-methylpyrimidine-4,6-diolu. Dinitromethan v odpadní směsi byl odstraněn termickým rozkladem nebo redukcí železem. Obsah dinitromethanu v reakční směsi byl stanoven sledován pomocí FTIR, UV-Vis nebo TLC. Bylo nastíněno možné využití dinitromethanu. Možné využití Termický rozklad odpadní reakční směsi byl sledován pomocí kalorimetrie (ARC).	dinitromethan; 2,2-dinitroethene-1,1-diamin; infračervená spektroskopie
eng	Synthesis of 2,2-dinitroethene-1,1-diamine from 2 methylpyrimidine-4,6-diol and treatment of the dinitromethane produced	2,2-Dinitroethene-1,1-diamine (FOX-7) was prepared from 2-methylpyrimidine-4,6-diol. Dinitromethane remaining in the spent acid was disposed of by thermal decomposition or reduction with iron. Dinitromethane content in reaction mixtures was monitored by FTIR, UV-Vis spectroscopy and thin layer chromatography (TLC). Possible reuse of dinitrome¬thane is discussed. The thermal decomposition of the spent acid was studied using accelerating rate calorimetry (ARC).	dinitromethan; 2,2-dinitroethene-1,1-diamine; infrared spectroscopy

Search