Publication detail

Extraction of Alkylphenols and Nonylphenol Mono and Diethoxylates from Water Using Magnetically modified Adsorbents

Year: 2008

Type of publication: článek v odborném periodiku

Name of source: Chromatographia

Publisher name: Springer

Page from-to: 1612-1617

Titles:

Language	Name	Abstract	Keywords
cze	Extrakce alkylfenolů a oxyethylenovaných nonylfenolů z vody pomocí magneticky modifikovaných sorbentů	Tato práce se zabývá jednoduchou extrakční technikou alkylfenolů a oxyethylenovaných nonylfenolů z vody. Pro extrakci těchto polutantů byla použita extrakce magnetickou tuhou fází, MSPE. Výsledky byly porovnány pomocí LLE.
eng	Extraction of Alkylphenols and Nonylphenol Mono and Diethoxylates from Water Using Magnetically modified Adsorbents	This paper presents a new simple method of extraction of alkylphenols (APs) and nonylphenol mono- and diethoxylates (NP1EO and NP2EO) from water. For the extraction of these pollutants, magnetic solid phase extraction (MSPE) was tested and the results were compared with liquid?liquid extraction (LLE). Different types of adsorbents, such as Chromosorb, Tenax, Porapak and Chezacarb were magnetically modified and used for the preconcentration and isolation of the target compounds. The following four extraction parameters were optimized: time of sorption, time of elution, volumes of elution solvents and number of repeated elutions. The target analytes were isolated from spiked distilled and tap water, real samples from the river Elbe and the reservoir Rozkos and also from water phase after biodegradation tests of oxyethylated nonylphenols. Extracts of pollutants were analyzed by capillary gas chromatography (GC). Detection limits of the method were between 0.7 and 1 lg L-1.	Gas chromatography;Magnetic Solid Phase Extraction;Nonylphenol monoethoxylates;and diethoxylates;Alkylphenols

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